The drug seizure came a month after the DRI recovered 260 kg of heroin worth Rs 1,300 crore during a raid at a container station near the Kandla port in Kutch district.
The team first arrested two persons, including a woman, and recovered around 5 gm of drugs from them, said SI Lakhimpur.
The NCB raid operation was conducted on Wednesday, said an official.
An SOG team arrested the accused duo with 238.4 gm of mephedrone, worth Rs 23.8 lakh.
Thirty-three kg of ganja and 1,060 pain relief tablets were recovered from the arrested persons, said an official.
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The accused has been booked under relevant sections of the Indian Penal Code (IPC) and the Narcotic Drugs and Psychotropic Substances (NDPS) Act.